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Lecturer(s)
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Gajzlerová Lenka, Ing. Ph.D.
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Krejčí Ondřej, Ing. Ph.D.
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Polášková Martina, doc. Ing. Ph.D.
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Course content
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1. Seminar: Introduction; materials, tools, instruments; laboratory procedure, operation; weighing, yield; laboratory records; tables. 2. Laboratory: Word safety, first aid; materials, tools, instruments; work with glass, assembling of the apparatus, laboratory instructions. 3. Seminar: Matter, weight, maintenance laws, volume and density. 4. Laboratory: Density determination, densimeter, flotation, pycnometer; sedimentation and decantation; raw material processing; plastics, polymers. 5. Seminar: Yield, theoretical yield, reaction range. Purity, contaminants. 6. Laboratory: Weighing; ceramics; heating, baths, flame, furnace; annealing, pigments preparation, lime burning. 7. Seminar: Solutions, concentration, dilution and mixing, calculations. 8. Laboratory: Work with liquids, common solvents, volume measuring, dosing, solutions preparation, purification, separation of the solutions components, filtration, precipitation, melting temperature, sublimation. 9. Seminar: Heterogeneous reactions, gases in the laboratories. 10. Laboratory: Work with gases, protective atmosphere, gases sources. 11. Seminar: Heat, heating and cooling; phase change, degrees of freedom, boiling point, evaporation, distillation. 12. Laboratory: Steam distillation, extraction, phases separation, refractive index. 13. Seminar: The history of the field. 14. Laboratory: Submissions, possibility of the substitution.
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Learning activities and teaching methods
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Monologic (Exposition, lecture, briefing), Dialogic (Discussion, conversation, brainstorming), Demonstration, Simple experiments
- Participation in classes
- 42 hours per semester
- Home preparation for classes
- 20 hours per semester
- Preparation for course credit
- 28 hours per semester
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| learning outcomes |
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| Knowledge |
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| Describe the laboratory equipment, laboratory glassware and instruments |
| Describe the laboratory equipment, laboratory glassware and instruments |
| Determine the mass, volume and density of liquids and solids |
| Determine the mass, volume and density of liquids and solids |
| Define yield, theoretical yield and response range |
| Define yield, theoretical yield and response range |
| Describe the phase change |
| Describe the phase change |
| Characterize methods of separating components of mixtures based on sublimation, precipitation, density and evaporation |
| Characterize methods of separating components of mixtures based on sublimation, precipitation, density and evaporation |
| Skills |
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| Basic skils required for work in laboratories and understands basic concepts for further study of chemistry and material technology |
| Basic skils required for work in laboratories and understands basic concepts for further study of chemistry and material technology |
| Assemble chemical apparatus |
| Assemble chemical apparatus |
| Select the appropriate type of laboratory glassware and equipment |
| Select the appropriate type of laboratory glassware and equipment |
| Work with gases and protective atmosphere |
| Work with gases and protective atmosphere |
| Separate the different components of mixtures on the basis of different chemical and physical properties |
| Separate the different components of mixtures on the basis of different chemical and physical properties |
| Prepare solutions, dilution and mixing |
| Prepare solutions, dilution and mixing |
| Describe the experiment and report it in a protocol |
| Describe the experiment and report it in a protocol |
| teaching methods |
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| Knowledge |
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| Dialogic (Discussion, conversation, brainstorming) |
| Dialogic (Discussion, conversation, brainstorming) |
| Monologic (Exposition, lecture, briefing) |
| Monologic (Exposition, lecture, briefing) |
| Skills |
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| Simple experiments |
| Simple experiments |
| Demonstration |
| Demonstration |
| assessment methods |
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| Knowledge |
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| Analysis of another type of paper written by the student (Casuistry, diary, plan ...) |
| Grade (Using a grade system) |
| Grade (Using a grade system) |
| Analysis of another type of paper written by the student (Casuistry, diary, plan ...) |
| Didactic test |
| Didactic test |
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Recommended literature
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-. dle doporučení vyučujícího.
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Titus Lucretius Carus: O přírodě, Plinius Starší: Kapitoly o přírodě, Vitruvius: Deset knih o architektuře - vše Antická knihovna. H.S. Cyrano de Bergerac: Cesta na měsíc ? Cesta do sluneční říše.
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GARLAND, C.W, NIBLER, J.W. SHOEMAKER, D.S. Experiments in Physical Chemistry. McGrawHill, 2009.
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Růžička, A. a kol. Laboratorní technika a cvičení z anorganické chemie. Brno: PřF MU, 1995.
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Sýkorová, D., Mastný, L. Návody pro laboratoře z anorganické chemie. Praha: VŠCHT, 2009.
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