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Lecturer(s)
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Vinter Štěpán, Ing. Ph.D.
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Šenkárová Lenka, Ing. Ph.D.
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Course content
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1. Introduction to structural and surface analysis, overview and classification of methods. 2. Atomic spectroscopy - revision of AAS, AES, XRF ICP-MS; elemental surface analysis. 3. Auger electron spectroscopy, X-ray fluorescence analysis, XRF, EDX, WDX. 4. Elemental surface analysis techniques - SIMS secondary ion mass spectrometry. 5. Techniques of surface microscopy, optical nanospectroscopy, infrared nanospectroscopy. 6. X-ray diffractometry. 7. Electron diffraction, neutron diffraction. 8. Overview of techniques of molecular analysis - IR, infrared microspectroscopy. 9. Overview of molecular analysis techniques - Raman spectroscopy - normal, resonance, Raman microspectroscopy. 10. NMR. 11. Comparison of methods. 12. Combined techniques. 13. Basics of thermal analysis. 14. Radioisotopic analysis.
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Learning activities and teaching methods
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- Preparation for course credit
- 25 hours per semester
- Participation in classes
- 70 hours per semester
- Home preparation for classes
- 30 hours per semester
- Preparation for examination
- 25 hours per semester
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| learning outcomes |
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| Knowledge |
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| list and explain the principle of structural and surface analysis - Atomic spectroscopy |
| list and explain the principle of structural and surface analysis - Atomic spectroscopy |
| list and explain the principle of structural and surface analysis - Molecular spectroscopy |
| list and explain the principle of structural and surface analysis - Molecular spectroscopy |
| list and explain the principle of structural and surface analysis - Techniques of surface microscopy |
| list and explain the principle of structural and surface analysis - Techniques of surface microscopy |
| list and explain the principle of structural and surface analysis - Diffraction techniques |
| list and explain the principle of structural and surface analysis - Diffraction techniques |
| Skills |
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| Interpretation of NMR spectra |
| Interpretation of NMR spectra |
| Interpretation of MS spectra |
| Interpretation of MS spectra |
| Interpretation of IR spectra |
| Interpretation of IR spectra |
| Interpretation of Raman spectra |
| Interpretation of Raman spectra |
| teaching methods |
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| Knowledge |
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| Lecturing |
| Lecturing |
| Dialogic (Discussion, conversation, brainstorming) |
| Dialogic (Discussion, conversation, brainstorming) |
| Skills |
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| Simple experiments |
| Simple experiments |
| Individual work of students |
| Individual work of students |
| assessment methods |
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| Knowledge |
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| Analysis of works made by the student (Technical products) |
| Analysis of works made by the student (Technical products) |
| Oral examination |
| Oral examination |
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Recommended literature
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Prezentace z přednášek.
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Houser, J., Novotný, L. Laboratorní cvičení ze speciálních metod instrumentální analýzy II. Brno : UTB, 2002. ISBN 80-214-1654-8.
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Churáček, J. Funkční analýza a identifikace organických látek - skriptum. Pardubice : VŠCHT, 1981.
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PAVIA,D. L. Introduction to Spectroscopy. 5th Ed.. Stamford: Cengage Learning, 2015. ISBN 978-1-285-46012-3.
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PETROZZI, S. Practical Instrumental Analysis: Methods, Quality Assurance and Laboratory Management.. Weinheim: Wiley VCH, 2013. ISBN 978-3-527-32951-9.
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ROBINSON, J.W. Undergraduate Instrumental Analysis. 7th Ed. Boca Raton: CRC Press, 2014. ISBN 978-1-4200-6135-2.
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ZÁRUBA, K. Analytická chemie. Díl 2.. Praha: VŠCHT, 2016. ISBN 978-80-7080-951-8.
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