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Lecturer(s)
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Janovský Petr, Ing. Ph.D.
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Šenkárová Lenka, Ing. Ph.D.
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Rouchal Michal, doc. Ing. Ph.D.
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Kimmel Roman, Ing. Ph.D.
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Course content
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1. Introduction to instrumental analysis, preparation of samples for analysis. 2. Data processing and evaluation, extraction, SPE. 3. Electroanalytical methods (potentiometry, polarography, voltammetry, conductometry, coulometry). 4. Electromigration methods (electrophoresis, isotachophoresis, isoelectric focusing). 5. Introduction to spectral methods, AES. 6. AAS, XRF. 7. UV-VIS, Fluorescence spectrometry. 8. IR, Raman spectrometry. 9. NMR, Nephelometry, Turbidimetry, Refractometry, Interferometry. 10. Mass spectrometry (MS). 11. Introduction to chromatography, TLC. 12. HPLC, UPLC, GPC. 13. IEC, affinity and chiral chromatography, GC. 14. SFC, quantitative and qualitative chromatography.
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Learning activities and teaching methods
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- Participation in classes
- 56 hours per semester
- Home preparation for classes
- 34 hours per semester
- Preparation for course credit
- 15 hours per semester
- Preparation for examination
- 15 hours per semester
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| learning outcomes |
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| Knowledge |
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| describe sample preparations for analysis |
| describe sample preparations for analysis |
| list and explain the principle of the electroanalytical method |
| list and explain the principle of the electroanalytical method |
| list and explain the principle of the electromigration method |
| list and explain the principle of the electromigration method |
| list and explain the principle of spectral methods |
| list and explain the principle of spectral methods |
| list and explain the principle of separation methods |
| list and explain the principle of separation methods |
| Skills |
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| familiarization with individual devices |
| familiarization with individual devices |
| teaching methods |
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| Knowledge |
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| Lecturing |
| Lecturing |
| Dialogic (Discussion, conversation, brainstorming) |
| Dialogic (Discussion, conversation, brainstorming) |
| Skills |
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| Simple experiments |
| Simple experiments |
| Practice exercises |
| Practice exercises |
| assessment methods |
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| Knowledge |
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| Analysis of works made by the student (Technical products) |
| Analysis of works made by the student (Technical products) |
| Oral examination |
| Oral examination |
| Grade (Using a grade system) |
| Grade (Using a grade system) |
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Recommended literature
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Holzbecher, Z., Churáček, J. Analytická chemie. Praha : SNTL, 1987.
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RUBINSON, K.A. Contemporary Instrumental Analysis.. Upper Saddle River: Prentice Hall, 2000. ISBN 137907265.
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SKOOG, D. Fundamentals of analytical chemistry, 9th ed.. Belmont: Brooks/Cole Cengage Learning, 2014. ISBN 978-0-495-55828-6.
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Willard, H. H. Instrumental methods of analysis. Belmont : Wadsworth Publishing, 1988. ISBN 0534081428.
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ZÁRUBA, K. Analytická chemie. Praha: VŠCHT Praha, 2016. ISBN 978-80-7080-950-1.
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