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Lecturer(s)
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Šenkárová Lenka, Ing. Ph.D.
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Vinter Štěpán, Ing. Ph.D.
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Course content
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1. Introduction to instrumental analysis, preparation of samples for analysis. 2. Data processing and evaluation, extraction, SPE. 3. Electrochemical methods (potentiometry, polarography, voltammetry, conductometry, coulometry). 4. Electromigration methods (electrophoresis, isotachoforesis, isoelectric focusing). 5. Introduction to spectral methods, AES. 6. AAS, XRF. 7. UV-VIS, fluorescence spectrometry. 8. IR, Raman spectroscopy. 9. NMR and nephelometry, turbidimetry, refractometry, interferometry. 10. Mass Spectrometry (MS). 11. Introduction to chromatography, TLC. 12. HPLC, UPLC, GPC. 13. IEC, affinity chromatography and chiral GC. 14. SFC, quantitative and qualitative chromatography.
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Learning activities and teaching methods
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Lecturing, Monologic (Exposition, lecture, briefing)
- Participation in classes
- 42 hours per semester
- Home preparation for classes
- 13 hours per semester
- Preparation for course credit
- 10 hours per semester
- Preparation for examination
- 25 hours per semester
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| prerequisite |
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| Knowledge |
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| The knowledge of inorganic, organic, analytical chemistry and work safety. |
| The knowledge of inorganic, organic, analytical chemistry and work safety. |
| learning outcomes |
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| describe sample preparations for analysis |
| describe sample preparations for analysis |
| list and explain the principle of the electroanalytical method |
| list and explain the principle of the electroanalytical method |
| list and explain the principle of the electromigration method |
| list and explain the principle of the electromigration method |
| list and explain the principle of spectral methods |
| list and explain the principle of spectral methods |
| ist and explain the principle of separation methods |
| ist and explain the principle of separation methods |
| Skills |
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| design and calculate sample preparation |
| design and calculate sample preparation |
| process and calculate the measurement results of electroanalytical methods |
| process and calculate the measurement results of electroanalytical methods |
| process and calculate the measurement results of spectral methods |
| process and calculate the measurement results of spectral methods |
| process and calculate the measurement results of separation methods |
| process and calculate the measurement results of separation methods |
| teaching methods |
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| Knowledge |
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| Monologic (Exposition, lecture, briefing) |
| Lecturing |
| Monologic (Exposition, lecture, briefing) |
| Lecturing |
| Skills |
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| Dialogic (Discussion, conversation, brainstorming) |
| Dialogic (Discussion, conversation, brainstorming) |
| Practice exercises |
| Practice exercises |
| assessment methods |
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| Knowledge |
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| Written examination |
| Written examination |
| Oral examination |
| Grade (Using a grade system) |
| Grade (Using a grade system) |
| Oral examination |
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Recommended literature
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Holzbecher, Z., Churáček, J. Analytická chemie. Praha : SNTL, 1987.
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Rubinson, Kenneth A. Contemporary instrumental analysis. Upper Saddle River : Prentice Hall, 2000. ISBN 137907265.
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SKOOG, D. Fundamentals of analytical chemistry, 9th ed.. Belmont: Brooks/Cole Cengage Learning, 2014. ISBN 978-0-495-55828-6.
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Willard, H. H. Instrumental methods of analysis. Belmont : Wadsworth Publishing, 1988. ISBN 0534081428.
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ZÁRUBA,K. Analytická chemie. Praha: VŠCHTv Praze, 2016. ISBN 978-80-7080-950-1.
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