Course: Analytical Chemistry Laboratory

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Course title Analytical Chemistry Laboratory
Course code TUIOZP/TP3LA
Organizational form of instruction Tutorial
Level of course Bachelor
Year of study not specified
Semester Winter
Number of ECTS credits 3
Language of instruction Czech
Status of course Compulsory
Form of instruction Face-to-face
Work placements This is not an internship
Recommended optional programme components None
Lecturer(s)
  • Šenkárová Lenka, Ing. Ph.D.
  • Bednařík Vratislav, doc. Ing. Ph.D.
  • Vinter Štěpán, Ing. Ph.D.
Course content
1. Argentometric determination of chloride. Calculation of equilibrium concentrations of ions at coagulation reactions. 2. Determination of copper by iodometry and electrogravimetry. 3. Direct spectrofotometric determination of a dye. 4. Measurement of proteolytic reaction curve. Determination of strong acids by potentiometric titration. 5. Conductometric determination of strong acids. 6. Manganometric determination of oxalic acid. 7. Qualitative analysis of inorganic cations and anions. 8. Bromatometric determination of phenol. 9. Determination of OH- a CO3/2- side by side according to Winkler. 10. Proteolytic titration curve. Determination of OH- a CO3/2- side by side according to Warder. 11. Determination of vitamin C content in a commercial product by bromatometry and voltametry. 12. Chelatometric determination of Ca2+ and Mg2+ salts, water hardness.

Learning activities and teaching methods
Simple experiments
  • Participation in classes - 42 hours per semester
  • Home preparation for classes - 24 hours per semester
  • Preparation for course credit - 24 hours per semester
prerequisite
Knowledge
Knowledge of general, inorganic and organic chemistry, mathematics and physics.
Knowledge of general, inorganic and organic chemistry, mathematics and physics.
Ability to pursue all calculations by the help of calculators.
Ability to pursue all calculations by the help of calculators.
Ability to respect the specified routine.
Ability to respect the specified routine.
learning outcomes
The necessary knowledge for the laboratory exercise is obtained (and stated in the form) in the course Analytical Chemistry.
The necessary knowledge for the laboratory exercise is obtained (and stated in the form) in the course Analytical Chemistry.
Skills
accurate weighing using analytical scales
accurate weighing using analytical scales
practical implementation of quantitative chemical analysis
practical implementation of quantitative chemical analysis
measurement of the pH value using a pH-meter
measurement of the pH value using a pH-meter
measurement using a UV-VIS spectrophotometer
measurement using a UV-VIS spectrophotometer
written processing of analysis results in the form of a protocol
written processing of analysis results in the form of a protocol
teaching methods
Knowledge
Monologic (Exposition, lecture, briefing)
Monologic (Exposition, lecture, briefing)
Dialogic (Discussion, conversation, brainstorming)
Dialogic (Discussion, conversation, brainstorming)
Skills
Simple experiments
Simple experiments
Practice exercises
Practice exercises
assessment methods
Knowledge
Grade (Using a grade system)
Systematic observation of the student
Systematic observation of the student
Analysis of the student's performance
Analysis of the student's performance
Grade (Using a grade system)
Analysis of works made by the student (Technical products)
Analysis of works made by the student (Technical products)
Recommended literature
  • HA RVEY, D. Modern Analytical Chemistry. McGraw Hill, London, 2000. ISBN 0-07-237547-7.
  • Holzbecher, Z., Churáček, J. a kol. Analytická chemie. Praha : SNTL, 1987.
  • Kuster-Thiel. Chemicko-analytické výpočetní tabulky. Praha : Academia, 1988.
  • SÝKORA, V. Chemicko-analytické tabulky. Praha: SNTL, 1976.
  • Vondruška, Milan. Analytická chemie. 1. vyd. Zlín : Univerzita Tomáše Bati, 2004. ISBN 8073182122.


Study plans that include the course
Faculty Study plan (Version) Category of Branch/Specialization Recommended year of study Recommended semester