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Lecturer(s)
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Šenkárová Lenka, Ing. Ph.D.
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Vinter Štěpán, Ing. Ph.D.
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Course content
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1. Introduction, overview and classification of methods. Elementary qualitative and quantitative analysis. 2. Distillation. 3. Sublimation, foam division, zone melting. 4. Extraction. 5. Membrane separations. 6. Electromigration methods. 7. Isoelectric focusing, isotachophoresis. 8. Capillary electrophoresis, capillary zone electrophoresis, micellar electrokinetic chromatography, capillary gel electrophoresis, capillary isoelectric focusing, capillary isotachophoresis, capillary electrochromatography. 9. Theory of chromatography. 10. GC. 11. LC. 12. IPC, SEC, GPC, Affinity, HIC, Chiral, IC, SMB. 13. SFC, chromatofocusing. 14. MS.
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Learning activities and teaching methods
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- Preparation for examination
- 210 hours per semester
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| learning outcomes |
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| Knowledge |
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| list and explain the principle of spectral methods |
| list and explain the principle of spectral methods |
| list and explain the principle of the electromigration method |
| list and explain the principle of the electromigration method |
| list and explain the principle of elementary analyses |
| list and explain the principle of elementary analyses |
| explain the principle of mass analysis |
| explain the principle of mass analysis |
| Skills |
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| perform element analysis in samples using spectroscopic methods, e.g. AAS, AMA |
| perform element analysis in samples using spectroscopic methods, e.g. AAS, AMA |
| perform analysis in samples using separation methods, e.g. GC, HPLC |
| perform analysis in samples using separation methods, e.g. GC, HPLC |
| perform analysis in samples using electroanalytical methods, e.g. ISE, Voltammetry |
| perform analysis in samples using electroanalytical methods, e.g. ISE, Voltammetry |
| perform molecular analysis in samples using spectroscopic methods, e.g. IR |
| perform molecular analysis in samples using spectroscopic methods, e.g. IR |
| teaching methods |
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| Knowledge |
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| Lecturing |
| Lecturing |
| Dialogic (Discussion, conversation, brainstorming) |
| Dialogic (Discussion, conversation, brainstorming) |
| Skills |
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| Simple experiments |
| Simple experiments |
| Practice exercises |
| Practice exercises |
| assessment methods |
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| Knowledge |
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| Didactic test |
| Didactic test |
| Analysis of works made by the student (Technical products) |
| Analysis of works made by the student (Technical products) |
| Oral examination |
| Oral examination |
| Grade (Using a grade system) |
| Grade (Using a grade system) |
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Recommended literature
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Prezentace z přednášek..
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Boček, P., Deml, M., Gebauer, P., Dolník, V. Analytická kapilární izotachoforéza. Praha : Academia, 1987.
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Holzbecher, Z., Churáček, J. a kol. Analytická chemie. Praha : SNTL, 1987.
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Houser, J., Novotný, L. Laboratorní cvičení ze speciálních metod instrumentální analýzy II. Brno : UTB, 2002. ISBN 80-214-1654-8.
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CHURÁČEK, J. Funkční analýza a identifikace organických látek.. Skriptum. Pardubice: VŠCHT, 1981.
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PETROZZI, S. Practical Instrumental Analysis: Methods, Quality Assurance and Laboratory Management. Weinheim: Wiley-VCH, 2013. ISBN 978-3-527-32951-9.
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ROBINSON, J.W. Undergraduate Instrumental Analysis. 7th Ed. Boca Raton: CRC Press, 2014. ISBN 978-1-4200-6135-2.
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ZÁRUBA, K. Analytická chemie. Díl 2.. Praha: VŠCHT, 2016. ISBN 978-80-7080-951-8.
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