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Lecturer(s)
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Dastychová Lenka, RNDr. Ph.D.
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Course content
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1. Functions of valves and taps, apparatus tightness testing, work with glass (bending, sealing, grinding), use of various materials as a part of chemical apparatus. 2. Assembly of inert gas equipment (inert gases, manifold, desiccants, vacuum pump); preparation of samples for NMR and MS. 3. Various methods of reduced pressure distillation; types of dryers, preparation of drying columns and possibilities of their use; drying solvents. 4. Reduced pressure sublimation, analysis of raw material and sublimation products. 5. Synthesis of a selected compound in an inert atmosphere; design of synthetic procedure, product analysis and reaction monitoring. 6. Analysis and evaluation of measured data, discussion.
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Learning activities and teaching methods
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- Participation in classes
- 56 hours per semester
- Home preparation for classes
- 10 hours per semester
- Preparation for course credit
- 24 hours per semester
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| prerequisite |
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| Knowledge |
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| Work with knowledge from all completed chemical and physical lerning courses. |
| Work with knowledge from all completed chemical and physical lerning courses. |
| Skills |
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| Use laboratory procedures at the level of completed chemical subjects. |
| Use laboratory procedures at the level of completed chemical subjects. |
| learning outcomes |
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| Knowledge |
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| Distribution of technical gases |
| Distribution of technical gases |
| Knowledge of different types of laboratory materials (types of glass, plastics) |
| In submitted protocols. |
| In submitted protocols. |
| Knowledge of different types of laboratory materials (types of glass, plastics) |
| Types of desiccants and their use |
| Types of desiccants and their use |
| Knowledge of glassware for an inert atmosphere |
| Knowledge of glassware for an inert atmosphere |
| Skills |
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| Using more complex assemblies for chemical synthesis |
| Using more complex assemblies for chemical synthesis |
| Working with pressure cylinders |
| Working with pressure cylinders |
| Working with an inert atmosphere in chemical apparatus |
| Working with an inert atmosphere in chemical apparatus |
| Sublimation under reduced pressure |
| Sublimation under reduced pressure |
| Simple repairs of glassware |
| Simple repairs of glassware |
| Drying of solvents |
| Drying of solvents |
| teaching methods |
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| Knowledge |
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| Demonstration |
| Demonstration |
| Dialogic (Discussion, conversation, brainstorming) |
| Dialogic (Discussion, conversation, brainstorming) |
| Simple experiments |
| Simple experiments |
| Students working in pairs |
| Students working in pairs |
| Dealing with situational issues - learning in situations |
| Dealing with situational issues - learning in situations |
| Teamwork |
| Teamwork |
| Skills |
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| Simple experiments |
| Simple experiments |
| Practice exercises |
| Practice exercises |
| Demonstration |
| Demonstration |
| Training in motion and work skills |
| Training in motion and work skills |
| Students working in pairs |
| Students working in pairs |
| Teamwork |
| Teamwork |
| Experience (self-experience) |
| Experience (self-experience) |
| assessment methods |
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| Knowledge |
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| Analysis of works made by the student (Technical products) |
| Analysis of works made by the student (Technical products) |
| Grade (Using a grade system) |
| Grade (Using a grade system) |
| Analysis of another type of paper written by the student (Casuistry, diary, plan ...) |
| Analysis of another type of paper written by the student (Casuistry, diary, plan ...) |
| Analysis of the student's performance |
| Analysis of the student's performance |
| Systematic observation of the student |
| Systematic observation of the student |
| Essay |
| Essay |
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Recommended literature
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Armarego, Wilfred L. F. Purification of laboratory chemicals. 5th ed. Amsterdam : Butterworth Heinemann, 2003. ISBN 750675713.
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D. F. Shriver, M. A. Drezdzon. The Manipulation of Air Sensitive Compounds. New York, 1986. ISBN 0-471-86773-X.
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J. D. Woolins a kol. Inorganic Experiments. Weinheim, VCH Verlagsgeselschaft mbH, 1994. ISBN 3-527-29253-5.
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NEUMAYEROVÁ, Z. Speciální laboratorní technika. FCH, ÚCHM, bakalářská práce. Vedoucí práce: L. Richtera. Brno: VUT, 2008.
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P. H. Plesch. High Vacuum Techniques for Chemical Syntheses and Measurements. Cambridge University Press, 2005. ISBN 9780521675475.
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PŘÍHODA, J. a kol. Laboratorní technika - Příručka pro začínajícího chemika. Brno: MU Brno, 2012.
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