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Lecturer(s)
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Dastychová Lenka, RNDr. Ph.D.
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Course content
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1. Functions of valves and taps, apparatus tightness testing, work with glass (bending, sealing, grinding), use of various materials as a part of chemical apparatus. 2. Assembly of inert gas equipment (inert gases, manifold, desiccants, vacuum pump); preparation of samples for NMR and MS. 3. Various methods of reduced pressure distillation; types of dryers, preparation of drying columns and possibilities of their use; drying solvents. 4. Reduced pressure sublimation, analysis of raw material and sublimation products (TLC, NMR, MS). 5. Synthesis of an organophosphorus compound in an inert atmosphere; design of synthetic procedure, product analysis and reaction monitoring (Tt, NMR, MS). 6. Preparation of complex compounds of nickel or tin in the inert atmosphere, isolation and analysis of products (NMR). 7. Analysis and evaluation of measured data, discussion.
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Learning activities and teaching methods
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- Preparation for course credit
- 24 hours per semester
- Home preparation for classes
- 10 hours per semester
- Participation in classes
- 56 hours per semester
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| prerequisite |
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| Knowledge |
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| Work with knowledge from all completed chemical and physical lerning courses. |
| Work with knowledge from all completed chemical and physical lerning courses. |
| Skills |
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| Use laboratory procedures at the level of completed chemical subjects. |
| Use laboratory procedures at the level of completed chemical subjects. |
| learning outcomes |
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| Knowledge |
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| In submitted protocols. |
| In submitted protocols. |
| Distribution of technical gases |
| Distribution of technical gases |
| Knowledge of different types of laboratory materials (types of glass, plastics) |
| Knowledge of different types of laboratory materials (types of glass, plastics) |
| Types of desiccants and their use |
| Types of desiccants and their use |
| Knowledge of glassware for an inert atmosphere |
| Knowledge of glassware for an inert atmosphere |
| Skills |
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| by continuous performance of assigned tasks |
| by continuous performance of assigned tasks |
| by active solving of assigned problems during the course |
| by active solving of assigned problems during the course |
| Using more complex assemblies for chemical synthesis |
| Using more complex assemblies for chemical synthesis |
| by practical demonstration of the required activities |
| by practical demonstration of the required activities |
| Working with pressure cylinders |
| Working with pressure cylinders |
| Working with an inert atmosphere in chemical apparatus |
| Working with an inert atmosphere in chemical apparatus |
| Sublimation under reduced pressure |
| Sublimation under reduced pressure |
| Simple repairs of glassware |
| Simple repairs of glassware |
| Drying of solvents |
| Drying of solvents |
| teaching methods |
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| Knowledge |
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| Demonstration |
| Demonstration |
| Dialogic (Discussion, conversation, brainstorming) |
| Dialogic (Discussion, conversation, brainstorming) |
| Simple experiments |
| Simple experiments |
| Students working in pairs |
| Students working in pairs |
| Teamwork |
| Teamwork |
| Experience (self-experience) |
| Experience (self-experience) |
| Skills |
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| Simple experiments |
| Simple experiments |
| Practice exercises |
| Practice exercises |
| Demonstration |
| Demonstration |
| Training in motion and work skills |
| Training in motion and work skills |
| Students working in pairs |
| Students working in pairs |
| Teamwork |
| Teamwork |
| Experience (self-experience) |
| Experience (self-experience) |
| assessment methods |
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| Knowledge |
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| Analysis of works made by the student (Technical products) |
| Analysis of works made by the student (Technical products) |
| Grade (Using a grade system) |
| Grade (Using a grade system) |
| Analysis of another type of paper written by the student (Casuistry, diary, plan ...) |
| Analysis of another type of paper written by the student (Casuistry, diary, plan ...) |
| Analysis of the student's performance |
| Analysis of the student's performance |
| Systematic observation of the student |
| Systematic observation of the student |
| Essay |
| Essay |
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Recommended literature
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Armarego, Wilfred L. F. Purification of laboratory chemicals. 5th ed. Amsterdam : Butterworth Heinemann, 2003. ISBN 750675713.
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D. F. Shriver, M. A. Drezdzon. The Manipulation of Air Sensitive Compounds. New York, 1986. ISBN 0-471-86773-X.
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J. D. Woolins a kol. Inorganic Experiments. Weinheim, VCH Verlagsgeselschaft mbH, 1994. ISBN 3-527-29253-5.
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NEUMAYEROVÁ, Z. Speciální laboratorní technika. FCH, ÚCHM, bakalářská práce. Vedoucí práce: L. Richtera. Brno: VUT, 2008.
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P. H. Plesch. High Vacuum Techniques for Chemical Syntheses and Measurements. Cambridge University Press, 2005. ISBN 9780521675475.
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PŘÍHODA, J. a kol. Laboratorní technika - Příručka pro začínajícího chemika. Brno: MU Brno, 2012.
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