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Lecturer(s)
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Kuřitka Ivo, prof. Ing. et Ing. Ph.D. et Ph.D.
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Urbánek Pavel, Ing. PhD.
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Hanulíková Barbora, Ing. Ph.D.
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Ševčík Jakub, Ing. Ph.D.
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Škoda David, Mgr. Ph.D.
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Yadav Raghvendra Singh, Dr.
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Course content
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1. Principles of spectrometry. 2. Basic instumentation - source, dispersion systém, detection. 3. Quantification, limitations and error. 4. X-Ray difractometry. 5. Atomic absorption spectrometry, refractometry, polarimetry, turbidimetry. 6. UV VIS absorption spectrometry. 7. Fluorimetry. 8. IR absorption spectrometry I. 9. IR absorption spectrometry II. 10. Raman spectrometry. 11. Mass specrometry. 12. NMR. 13. Photoelectron spectroscopy, EPR. 14. Spectrometry in electron microscopy.
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Learning activities and teaching methods
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Lecturing, Dialogic (Discussion, conversation, brainstorming), Demonstration, Projection (static, dynamic), Simple experiments, Teamwork
- Preparation for course credit
- 120 hours per semester
- Participation in classes
- 56 hours per semester
- Home preparation for classes
- 14 hours per semester
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| prerequisite |
|---|
| Knowledge |
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| Basic knowledge of university courses in physics and chemistry common to technical universities. |
| Basic knowledge of university courses in physics and chemistry common to technical universities. |
| Skills |
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| Prepare solutions of given concentrations |
| Prepare solutions of given concentrations |
| Use text and table editor, create a graph displaying data (axes x-y) |
| Use text and table editor, create a graph displaying data (axes x-y) |
| learning outcomes |
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| Knowledge |
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| The student understands and can explain the physical principle of measurement methods and investigated phenomena. |
| The student understands and can explain the physical principle of measurement methods and investigated phenomena. |
| He/she has knowledge of measurement instrumentation, can describe it and explain the function of the basic components of the spectrometer. |
| He/she has knowledge of measurement instrumentation, can describe it and explain the function of the basic components of the spectrometer. |
| He/she is oriented in the basic requirements for sample preparation, he can describe them, give examples and justify them. |
| He/she is oriented in the basic requirements for sample preparation, he can describe them, give examples and justify them. |
| He/she knows and can describe the typical output from the measurement and the methods of presentation of the obtained data, and he/she can interpret typical spectra. |
| He/she knows and can describe the typical output from the measurement and the methods of presentation of the obtained data, and he/she can interpret typical spectra. |
| He/she has an overview of the applications of individual methods and can suggest which method he/she would use to analyze a given sample. |
| He/she has an overview of the applications of individual methods and can suggest which method he/she would use to analyze a given sample. |
| Skills |
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| The student can prepare samples and measure spectra using basic methods. |
| The student can prepare samples and measure spectra using basic methods. |
| The student can use basic spectrometric methods and suggest how he/she would use them to solve typical questions after sample composition or analyte concentration. |
| The student can use basic spectrometric methods and suggest how he/she would use them to solve typical questions after sample composition or analyte concentration. |
| The student is able to process, present and interpret experimental data. |
| The student is able to process, present and interpret experimental data. |
| teaching methods |
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| Knowledge |
|---|
| Lecturing |
| Lecturing |
| Demonstration |
| Demonstration |
| Projection (static, dynamic) |
| Projection (static, dynamic) |
| Practice exercises |
| Practice exercises |
| Skills |
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| Simple experiments |
| Simple experiments |
| Teamwork |
| Teamwork |
| Dialogic (Discussion, conversation, brainstorming) |
| Dialogic (Discussion, conversation, brainstorming) |
| assessment methods |
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| Knowledge |
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| Written examination |
| Written examination |
| Oral examination |
| Oral examination |
| Analysis of works made by the student (Technical products) |
| Analysis of works made by the student (Technical products) |
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Recommended literature
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Organic structural spectroscopy. Upper Saddle River, N.J : Prentice Hall, 1998. ISBN 0-13-258690-8.
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Böhm, Stanislav. Strukturní analýza organických sloučenin. 1. vyd. Praha : VŠCHT, 1995. ISBN 8070802359.
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LAKOWICZ, J.R. Principles of fluorescence spectroscopy. . 3rd ed. New York: Springer, 2006. ISBN 9780387312781.
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NĚMCOVÁ, I.; ČERMÁKOVÁ, L.; RYCHLOVSKÝ, P. Spektrometrické analytické metody I. 2. vyd. Praha: Karolinum, 2004. ISBN 80-246-0776-X.
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NĚMCOVÁ, I.; ENGST, P.; JELÍNEK, I.; RYCHLOVSKÝ, P.; SEJBAL, J. Spektrometrické analytické metody II. Praha: Karolinum, 1998.
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ZERBI, G. Modern polymer spectroscopy. Weinheim ; Chichester, 1999. ISBN 3527296557.
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