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Lecturer(s)
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Kimmel Roman, Ing. Ph.D.
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Rouchal Michal, doc. Ing. Ph.D.
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Dastychová Lenka, RNDr. Ph.D.
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Vícha Robert, doc. Mgr. Ph.D.
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Prucková Zdeňka, Ing. Ph.D.
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Barbuščáková Zuzana, Mgr.
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Course content
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- Ethyl acetate. - 1-bromobutane. - 9,10-anthraquinone. - Acetanilide. - Aminolyses of 1-chloro-2,4-dinitrobenzene with an aromatic amine. - 4-nitroaniline. - Acetylsalicylic acid. - Terc-butylchloride. - Soxhlet extraction of plant leafs pigments. - 2-hydroxy-5-methyl-4'-nitroazobenzene. - Butyl acetate - green apple flavour. - Triphenylmethanol. - Dibenzylidenacetone. - 2,4,5-triphenylimidazole. - Dimerization of 2,4,5-triphenylimidazole. - Isolation of cloves essence. - Piperine - isolation of pepper alcaloid. - Methylparabene - Fisher esterification. - Cinnamic acid - Knoevenagel synthesis. - Methyl cinnamate - cinnamon flavour.
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Learning activities and teaching methods
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Simple experiments
- Participation in classes
- 42 hours per semester
- Preparation for course credit
- 15 hours per semester
- Home preparation for classes
- 33 hours per semester
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| learning outcomes |
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| Skills |
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| perform intermediate organic synthesis reactions |
| perform intermediate organic synthesis reactions |
| apply laboratory operations, such as extraction, Soxhlet extraction, distillation, azeotropic distillation, steam distillation, crystallization, filtration, and suction. |
| apply laboratory operations, such as extraction, Soxhlet extraction, distillation, azeotropic distillation, steam distillation, crystallization, filtration, and suction. |
| use basic spectral methods to characterize organic compounds using refraction index and melting point measurements, thin layer chromatography etc. |
| use basic spectral methods to characterize organic compounds using refraction index and melting point measurements, thin layer chromatography etc. |
| teaching methods |
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| Knowledge |
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| Dialogic (Discussion, conversation, brainstorming) |
| Dialogic (Discussion, conversation, brainstorming) |
| Methods for working with texts (Textbook, book) |
| Methods for working with texts (Textbook, book) |
| Skills |
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| Simple experiments |
| Simple experiments |
| Practice exercises |
| Practice exercises |
| assessment methods |
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| Knowledge |
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| Grade (Using a grade system) |
| Analysis of works made by the student (Technical products) |
| Analysis of works made by the student (Technical products) |
| Grade (Using a grade system) |
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Recommended literature
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http://www.chemie.utb.cz/rvicha/Loch/loch.php.
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Harwood L. M., Moody C. J., Percy J. M. Experimental Organic Chemistry. Oxford, Blackwell Publishing, 1999. ISBN 978-0-632-04819-9.
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Kafka, S. Cvičení z chemie. Brno : VUT, 1999.
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Vícha R., Mrkvička V. Laboratorní cvičení z chemie. Zlín: Univerzita Tomáše Bati, 2007. ISBN 978-80-7318-595-4.
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Vícha, Robert. Laboratorní cvičení z chemie : bezpečnost práce v chemické laboratoři, laboratorní technika, laboratorní úlohy z anorganické chemie, laboratorní úlohy z organické chemie. Vyd. 1. Zlín : Univerzita Tomáše Bati ve Zlíně, 2007. ISBN 978-80-7318-595-4.
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