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Lecturer(s)
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Bednařík Vratislav, doc. Ing. Ph.D.
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Course content
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1. Characteristics, classification and methods of chemical analysis, fundamentals of qualitative chemical analysis. 2. Expressing the concentration of substances in solution, dilution and mixing solutions. 3. Proteolytic balance in aqueous solutions, the strength of acids and bases, buffers, pH calculations. 4. Coagulation balance, slightly soluble electrolytes, solubility calculations. 5. Redox equilibria, redox potential, quantification of redox reactions. 6. Complex equilibrium constants of complexes, chelatometry, amphoteric metals. 7. Volumetric analysis, standard solution, primary and secondary standards, standard solution, the theoretical course of the titration curve, selection of color indicator, the calculation of the analyte in the sample. 8. Gravimetric analysis, sequence, selection of coagulants, the calculation of the analyte in the sample, the determination of dry matter. 9. Potentiometry, types of electrodes, standard hydrogen electrode, direct potentiometry, potentiometric titration, potentiometric pH measurements. 10. Conductometry, conductivity of the electrolyte, conductivity measurement principle, direct conductometry, conductometric titration. 11. Photometry, spectrometric methods, absorbance, absorption spectrum, direct photometry, photometric titration. 12. Processing the results of the analysis and evaluation of analytical procedures, the results of chemical analysis of errors, precision and accuracy, statistical processing of results of chemical analysis, process calibration dependence. 13. Qualitative chemical analysis of inorganic substances, the evidence selected cations and anions. 14. Basics of qualitative chemical analysis of organic compounds.
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Learning activities and teaching methods
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Lecturing, Monologic (Exposition, lecture, briefing), Demonstration, Practice exercises
- Participation in classes
- 16 hours per semester
- Preparation for examination
- 30 hours per semester
- Home preparation for classes
- 44 hours per semester
- Preparation for course credit
- 30 hours per semester
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| prerequisite |
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| Knowledge |
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| Knowledge of general, inorganic and organic chemistry, mathematics and physics. |
| Knowledge of general, inorganic and organic chemistry, mathematics and physics. |
| Ability to perform all calculations using a calculator. |
| Ability to perform all calculations using a calculator. |
| learning outcomes |
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| Students learn the following concepts, calculations and skills: - Number of individual chemical - Concentration of solution, dilution, mixing solutions - PH of aqueous solutions of acids, bases, salts, buffers - Solubility of slightly soluble electrolytes, factors affecting solubility - Electrochemical potential, the electrodes used in analytical chemistry - Complexing reaction, the stability constants of complexes - Basics of qualitative chemical analysis - Basics of quantitative chemical analysis - Volumetric analysis, preparation of volumetric solutions, standardization - Basics of optical methods of chemical analysis, spectrophotometry - Basics of electrochemical methods of chemical analysis, potentiometry, conductometry - Gravimetry, electrogravimetry - Statistical evaluation of results of chemical analysis |
| Students learn the following concepts, calculations and skills: - Number of individual chemical - Concentration of solution, dilution, mixing solutions - PH of aqueous solutions of acids, bases, salts, buffers - Solubility of slightly soluble electrolytes, factors affecting solubility - Electrochemical potential, the electrodes used in analytical chemistry - Complexing reaction, the stability constants of complexes - Basics of qualitative chemical analysis - Basics of quantitative chemical analysis - Volumetric analysis, preparation of volumetric solutions, standardization - Basics of optical methods of chemical analysis, spectrophotometry - Basics of electrochemical methods of chemical analysis, potentiometry, conductometry - Gravimetry, electrogravimetry - Statistical evaluation of results of chemical analysis |
| Skills |
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| calculate and propose the solution preparation procedure |
| calculate and propose the solution preparation procedure |
| calculate the result of chemical analysis |
| calculate the result of chemical analysis |
| calculate the theoretical pH value of any aqueous solution |
| calculate the theoretical pH value of any aqueous solution |
| calculate the solubility of a poorly soluble substance |
| calculate the solubility of a poorly soluble substance |
| determine the expected course of the redox reaction |
| determine the expected course of the redox reaction |
| teaching methods |
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| Knowledge |
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| Lecturing |
| Monologic (Exposition, lecture, briefing) |
| Monologic (Exposition, lecture, briefing) |
| Lecturing |
| Skills |
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| Demonstration |
| Demonstration |
| Practice exercises |
| Practice exercises |
| assessment methods |
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| Knowledge |
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| Oral examination |
| Oral examination |
| Grade (Using a grade system) |
| Written examination |
| Grade (Using a grade system) |
| Analysis of the student's performance |
| Analysis of the student's performance |
| Systematic observation of the student |
| Systematic observation of the student |
| Written examination |
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Recommended literature
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HARVEY, D. Modern Analytical Chemistry. Mc Graw Hill, London, 2000. ISBN 0-07-237547-7.
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Holzbecher, Z., Churáček, J. a kol. Analytická chemie. Praha : SNTL, 1987.
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Kuster-Thiel. Chemicko-analytické výpočetní tabulky. Praha : Academia, 1988.
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Vondruška, Milan. Analytická chemie. 1. vyd. Zlín : Univerzita Tomáše Bati, 2004. ISBN 8073182122.
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Zýka, J. a kol. Analytická příručka I, Analytická příručka II. Praha : SNTL, 1980.
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